Induction Heat setting Nitinol

Induction Heat Setting Nitinol Wire in a Steel Fixture

Quick Answer

Induction heat setting of Nitinol heats a steel fixture that holds the Nitinol in the required shape, then quenches it, so the alloy remembers that shape.

In this HLQ case, a 0.005 in (0.13 mm) Nitinol wire sat in a shape etched on a steel fixture. A special four-turn internal and external helical coil, driven by a DW-UHF-6kW-I at 500 kHz, heated the fixture to 930 °F (500 °C). It was held for 2.5 minutes and then quenched in water. The wire was shaped as desired within 4 minutes, using less energy and time than oven heating.

External helical induction coil around a steel fixture with an internal coil for Nitinol heat setting
External helical coil around the steel fixture, with the internal coil in the drilled bore.

What is Induction Heat Setting of Nitinol?

Nitinol is held in the required shape by a steel fixture, die or mandrel. The fixture is heated by induction to the set point, held there, and then quenched, so the part keeps the shape for its shape-memory function.

The wire is very fine, so the fixture is what is heated. It passes heat to the wire in the same way an induction-heated susceptor does; see induction susceptor heating.

Item HLQ case data
Objective Heat a 0.005 in (0.13 mm) diameter Nitinol wire for a shape-setting application
Material Nitinol wire; steel fixture
Temperature 930 °F (500 °C)
Frequency 500 kHz
Equipment DW-UHF-6kW-I solid-state power supply with a remote heat station containing two 0.33 µF capacitors (0.66 µF total), plus a coil designed for this application
Coil Special four-turn internal and external helical coil
Hold time 2.5 minutes at the set point
Quench Fixture quenched in water immediately after the heat cycle
Results Parts made to shape-memory specification; wire shaped as desired within 4 minutes, using less energy and time than traditional oven heating

Key Applications

HLQ Nitinol heat setting cases: wire in steel fixture 500 °C, wire in tapered die 507 °C, stents on mandrel 510 °C, continuous wire about 427 °C
Application case chart: four published HLQ Nitinol heat-setting examples.
HLQ case Fixture / part Temperature Time
Nitinol wire in steel fixture (this page) Concentric steel cylinders with the shape etched on the inner OD 930 °F (500 °C) 2.5 min hold; shaped within 4 min
Nitinol wire in a tapered steel die 2 in (50.8 mm) tapered steel die inside a steel tube; wire tacked with instant adhesive Die heated to 945 °F (507.2 °C) 75 s heating; setting achieved in 15 s
Nitinol medical stents Stents on a mandrel 510 °C Set to size in two minutes
Continuous Nitinol wire Wire passing through an induction coil About 800 °F (426.7 °C) Continuous

Related HLQ pages: induction heat setting a shape memory alloy, induction heating for medical and dental applications and induction heating coil design.

Shape-set Nitinol wire parts after induction heat setting
Shape-set Nitinol wire parts.

Suitable Materials

Item Role Notes
Nitinol wire, Ø0.005 in (0.13 mm) Part to be shape-set Held in the shape etched on the fixture
Steel fixture Induction-heated part Modified to reduce thermal mass; inner cylinder drilled for the internal coil
Steel die / mandrel Induction-heated part in related cases Tapered die; stent mandrel
Water Quench medium Fixture quenched immediately after the heat cycle

Working Principle

Principle of induction heat setting Nitinol: DW-UHF-6kW-I, 0.66 µF heat station, internal and external helical coils, concentric steel fixture with Nitinol wire
Principle diagram: power supply, heat station, internal and external coils, concentric steel fixture and Nitinol wire.
  1. The DW-UHF-6kW-I drives a remote heat station (2 × 0.33 µF) at 500 kHz.
  2. The four-turn coil works on both sides of the fixture: inside the drilled bore of the inner cylinder and around the outer cylinder.
  3. Eddy currents heat the steel fixture: a 0.1 in (2.54 mm) thick hollow outer cylinder over a 1 in (25.4 mm) solid inner cylinder.
  4. The fixture brings the Nitinol wire in the etched shape to 930 °F (500 °C), and it is held there for 2.5 minutes.
  5. Quenching the fixture in water completes the shape setting.

Background: how an induction heater works.

Induction coil for heat setting Nitinol with internal and external windings
Coil arrangement for the Nitinol heat-setting fixture.

Technical Specifications

Parameter Value in the HLQ case
Nitinol wire diameter 0.005 in (0.13 mm)
Fixture outer cylinder Hollow, 0.1 in (2.54 mm) thick
Fixture inner cylinder Solid, 1 in (25.4 mm) diameter, drilled for the internal coil
Set point 930 °F (500 °C)
Hold time 2.5 minutes
Quench Water
Total time to shaped wire Within 4 minutes
Frequency 500 kHz
Power supply DW-UHF-6kW-I
Heat station capacitance 2 × 0.33 µF = 0.66 µF
Set-up measurement Thermocouple on the empty fixture

Recommended Model Selection

HLQ series Power Frequency Nitinol use
DW-UHF-6kW 6 kW 300–1100 kHz Heat-setting fixtures and dies (this case: DW-UHF-6kW-I at 500 kHz)
DW-UHF (other models) 4.5–60 kW By model Larger fixtures or higher output
DW-HF 15–160 kVA 20–80 kHz (15 kW: 30–100 kHz) Larger, heavier fixtures

Full model data: HLQ induction heating device models. Fixture mass and size decide the power, so the cycle is confirmed by test.

Process Workflow

Nitinol heat setting workflow: modify fixture, thermocouple test, load wire, coil in place, heat to 500 °C and hold 2.5 min, water quench, shape-set part
Process flow chart from the HLQ Nitinol case.
Step Action Case reference
1 Prepare the fixture Modified to reduce thermal mass; inner cylinder drilled for the coil
2 Establish the heating cycle Thermocouple test on the fixture without a part
3 Load the Nitinol Wire placed in the etched shape; outer cylinder slipped over
4 Position the coil Internal and external helical coil
5 Heat and hold To 930 °F (500 °C); hold 2.5 minutes
6 Quench Fixture quenched in water immediately
7 Unload the part Shaped to specification within 4 minutes

Cell layout

Nitinol heat-setting cell layout with DW-UHF-6kW-I, remote heat station, heating station, thermocouple, water quench and loading bench
Layout diagram (schematic, not to scale) of a Nitinol heat-setting cell.

Common Problems and Solutions

Problem Likely cause Solution
Fixture heats too slowly Fixture thermal mass too high Reduce the fixture mass, as was done in the case
Uneven fixture temperature Coil on one side only Use an internal and external coil
Cycle not repeatable Heating cycle not established Set the cycle first with a thermocouple on the empty fixture
Shape not retained Hold time or quench not followed Hold 2.5 min at the set point and quench immediately

Engineering Selection Guide

Factor What to confirm Why it matters
Nitinol part Wire, tube or stent size Sets the fixture design
Fixture, die or mandrel Geometry and thermal mass Sets power and heating time
Set point and hold For example, 930 °F (500 °C) for 2.5 min Shape-memory result
Quench Water quench after heating Completes the setting
Coil Internal, external or both Uniform fixture temperature
Coil engineering Turns, shape and fit to the fixture See understanding the skin effect

Advantages and Limitations

Advantages Limitations
Wire shaped within 4 minutes The fixture must be designed and tested
Less energy and time than traditional oven heating The coil is designed for each fixture
Heat delivered to the fixture zone The heating cycle must be established by test
Repeatable cycle once established Thermal mass affects cycle time

Why Choose HLQ?

Strength Evidence
Nitinol experience Wire-in-fixture, tapered die, stent mandrel and continuous wire examples
Fixture engineering Thermal mass reduced; coil inside and outside the fixture
DW-UHF power supplies DW-UHF-6kW: 300–1100 kHz
Test-based set-up Thermocouple cycle development before production
Medical industry Heat treatment of memory alloys for medical applications
Faster than ovens Less energy and time in the case

10 Core FAQs

1. What temperature is used to heat set Nitinol in this case?

930 °F (500 °C), held for 2.5 minutes.

2. How long does the cycle take?

The wire is shaped as desired within 4 minutes.

3. Why is the fixture heated instead of the wire?

The 0.13 mm wire is held in the etched shape on the steel fixture. Induction heats the fixture, and the fixture brings the wire to the set point.

4. Which coil was used?

A special four-turn internal and external helical coil.

5. Which equipment and frequency?

A DW-UHF-6kW-I with a remote heat station (2 × 0.33 µF), at 500 kHz.

6. What happens after heating?

The fixture is quenched in water immediately.

7. How was the heating cycle developed?

With a thermocouple on the fixture, without a part, during initial tests.

8. Why was the fixture modified?

To reduce its thermal mass. The inner cylinder was also drilled so the internal coil could be inserted.

9. What other Nitinol jobs has HLQ shown?

Wire set in a tapered steel die (945 °F in 75 s), stents set on a mandrel at 510 °C in two minutes, and continuous wire heating at about 800 °F.

10. How does it compare with an oven?

In the case, induction shaped the wire using less energy and time than traditional oven heating.

HLQ-Induction-Heat-Setting-Nitinol-Brochure

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