Laboratory Vacuum Furnace-Vacuum Heat Treatment Furnace-Vacuum Sintering Furnace

Description

In the demanding world of materials science, metallurgy, and high-tech manufacturing, the laboratory vacuum furnace has become an indispensable component for achieving high-purity, high-performance results. Also known as a vacuum heat treatment furnace, this specialized equipment creates a controlled, low-pressure environment for precise heat treatment, ensuring superior material properties and unmatched process reliability.

What is a Laboratory Vacuum Furnace?

A laboratory vacuum furnace is a high-temperature oven designed to perform heat treatment processes such as annealing, sintering, brazing, and degassing under vacuum or inert gas environments. By eliminating atmospheric gases like oxygen and moisture, vacuum furnaces prevent oxidation, contamination, and unwanted chemical reactions during thermal processing.

Key Features

  • Oxidation Prevention:ย The vacuum environment shields sensitive samples from air, ensuring pure, uncontaminated results.
  • Wide Temperature Range:ย Typical working temperatures span from 800ยฐC up to 2000ยฐC, with stable, programmable control.
  • Ultimate Vacuum Levels:ย State-of-the-art models reach vacuum as low as 7 ร— 10โปยณ Pa, suitable for even the most demanding processes.
  • Superior Temperature Uniformity:ย With uniformity as tight as ยฑ5ยฐC, these furnaces deliver consistent and reproducible results across the entire chamber.
  • User-Friendly Controls:ย Advanced PLC systems and touchscreen interfaces offer precision, automation, and data logging for process optimization.

Common Applications of Vacuum Heat Treatment Furnace

Laboratory vacuum furnaces are crucial across multiple industries and research sectors. Key applications include:

1. Heat Treatment of Alloys and Metals

Processes such as annealing, tempering, and stress relieving can be performed without the risk of oxide scale or internal contamination, especially important for aerospace components and specialty alloys.

2. Sintering of Advanced Materials

These furnaces are ideal for sintering magnetic materials, powder metallurgy products, ceramics, and composites. The vacuum or inert atmosphere ensures high density and superior purity, essential for cutting-edge electronics and magnetic applications.

3. Thermal Processing of Magnet Materials

Vacuum heat treatment is vital for materials like NdFeB and SmCo magnets, where the strict control of atmosphere and temperature dramatically affects magnetic properties and service life.

4. Brazing and Bonding

Joining complex and sensitive parts, such as those used in medical devices or high-vacuum systems, requires oxide-free, high-integrity bonding only achievable in a vacuum furnace.

5. Degassing & Purification

High vacuum and temperature combine to remove residual gases, moisture, and volatile contaminants from metals, ceramics, and functional materials โ€” critical for semiconductor and high-purity applications.

 

High Temperature Lab Vacuum Furnace, 2200โ„ƒ Max. High Vacuum Heat Treatment Furnace.

This high temperature Vacuum Furnace is cost-effective. Max. vacuum 7ร—10-4Pa. Excellent uniformity, precise control for vacuum sintering, brazing, annealing, tempering and hardening, etc. It is used for ceramic materials, ceramic-metal composites, refractory metals, and alloy materials, as well as vacuum brazing of alloy tools and superhard materials.

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High Temperature Vacuum Furnace Applications:

ยทย ย ย ย ย ย  Vacuum heat treatment โ€“ hardening, tempering, and annealing

ยทย ย ย ย ย ย  Vacuum brazing

ยทย ย ย ย ย ย  Sintering

ยทย ย ย ย ย ย  Degassing

Advantages of High Temperature Vacuum Furnace:

ยทย ย ย ย ย ย  No surface oxidation or discoloration

ยทย ย ย ย ย ย  Minimal distortion

ยทย ย ย ย ย ย  Flux free brazing

ยทย ย ย ย ย ย  Repeatable quality

ยทย ย ย ย ย ย  Clean, safe, quiet and efficient

All our vacuum furnaces can be used with either an inert gas or a reactive gas. The majority of products in our vacuum furnace range are available with either ceramic fiber, molybdenum, or graphite insulation. On request, a furnace with a graphite insulation chamber can be configured to safely operate at up to 2200ยฐC.

3 types of Furnace Chamber for optional

 

Vacuum System:

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โ… .ย Technical Specifications

Max. temperature

1200โ„ƒ (Heating wires)

1350โ„ƒ (Molybdenum strap heaters )

1400โ„ƒ (SiC heating elements)

1700โ„ƒ (MoSi heating elements)

2200โ„ƒ (Graphite heating element)

Furnace chamber insulation

1200โ„ƒ (Ceramic fiber board)

1350โ„ƒ (Molybdenum sheets and Stainless steel sheets )

1400โ„ƒ (Ceramic fiber board)

1700โ„ƒ (Ceramic fiber board)

2200โ„ƒ (Carbon felt)

Furnace structure

โ—Double layers Carbon steel casing with water cooling system to ensure the surface below 30โ„ƒ

โ— Furnace door inside is polished stainless steel

Working voltage

380Vย  50HZ ย 3Pย ย  (or according to your standard)

Max. power

5KWโ€“180KW

Temperature controlling

โ—ย  PLC or PID automatic control via SCR (Silicon Controlled Rectifier) power control with phase angle fired, current limiting resistor.
โ—ย ย 51 programmable segments for precise control of heating rate, cooling rate and dwell time.
โ—ย ย Built in PID Auto-Tune function with overheating & thermocouple broken protection.
โ—ย ย Over temperature protection and alarm allows for operation without an attendant.

Optional of temperature controlling

โ—ย ย Software (Furnace can beย operated by PC by installing aย control softwareย )
โ—ย ย Touch screen temperature controller

Temperature accuracy

ยฑ1โ„ƒ

Heating rate

Heating rate<20 โ„ƒ/min

Thermocouple

1200โ„ƒ (S type)

1350โ„ƒ (S type)

1700โ„ƒ (B type)

2200โ„ƒ (W-Re type)

Maximum vacuum

7ร—10-4Pa

Vacuum pump

โ— 10Pa with Double stages rotary pump

โ— 7ร—10-1Paย with Mechanical pump and Roots pump

โ—7ร—10-3Pa with Mechanical pump and Diffusion pump

โ—7ร—10-4Pa with Mechanical pump and Molecular pump

Warranty

โ—ย ย One year limited warranty with lifetime support. (Consumable parts such as heating elements and crucibles are not covered by the warranty, please order the replacement at related products)
โ—ย ย ATTENTION: Any damages caused by the use of corrosive and acidic gases are not under the coverage of One Year Limited Warranty.

Certifications

CE

โ…ก. Application Notes

Using Attentions

โ—ย ย Cooling rate shall also not exceed 5 โ„ƒ /min.
โ—ย ย Toxic or explosive gases are not recommended for use with this furnace without necessary safety controls and supervision.
โ—ย ย Small cracks may appear on the surface of the refractory ceramics over extended use.

 

Customized high temperature vacuum furnace as below: (other sizes can be customized)

Parameter Specification
Model DW-1200-M
Furnace Chamber Dimensions 600 ร— 600 ร— 2300 mm (Alumina Ceramic)
Maximum Working Temperature 1200ยฐC
Long-term Working Temperature 1100ยฐC
Temperature Uniformity ยฑ5ยฐC (within effective working zone)
Heating Rate 0-20ยฐC/min (adjustable)
Ultimate Vacuum 7ร—10โปยณ Pa
Vacuum System

Mechanical Pump: 25 L/s

Molecular Pump: 1500 L/s

Vacuum Gauge: Full-range ionization gauge

Power Supply 380V, Three-phase five-wire system, Rated Power: 60 kW
Heating Elements Molybdenum wire heaters with multi-zone control
Temperature Control

PID Controller with program segment control

Thermocouple: Type B

Cooling System

Water-cooled (20 L/min)

Closed-loop circulation system

Protective Gas High-purity Nโ‚‚/Ar (99.999% purity)
Control System

PLC automatic control

Touch screen HMI

Data logging and export function

Safety Protection Devices

Over-temperature protection

Over-pressure protection

Water flow protection

Power failure protection

Emergency stop

Magnetic Field Shielding High magnetic permeability alloy shielding
Overall Dimensions 1800 ร— 1500 ร— 2800 mm
Weight Approx. 3500 kg
Process Atmosphere Vacuum / Inert gas
Operation Mode Fully automatic/manual optional
Workpiece Specifications

Diameter: 4 mm

Length: up to 200 mm

Application Field

Magnetic materials sintering

High-performance permanent magnet preparation

Heating Wires High Temperature Vacuum Furnace up to 1200โ„ƒ

Model

Max Temp.

Chamber size
(WxHxD)

Heating element

Capacity

(L)

Power

(KW)

Vacuum

DW-12HVF-1

1200

100*100*100

Resistance wire

1

1.2

7*10-3Pa

DW-12HVF-5

1200

150*150*200

Resistance wire

4.5

3.5

7*10-3Pa

DW-12HVF-12

1200

200*200*300

Resistance wire

12

5

7*10-3Pa

DW-12HVF-36

1200

300*300*400

Resistance wire

36

12

7*10-3Pa

DW-12HVF-64

1200

400*400*600

Resistance wire

96

24

7*10-3Pa

DW-12HVF-125

1200

500*500*700

Resistance wire

175

36

7*10-3Pa

DW-12HVF-216

1200

600*600*900

Resistance wire

324

56

7*10-3Pa

 

 

 

 

Molybdenum Foil High Temperature Vacuum Furnace up toย 1350โ„ƒ

Model

Chamber size

Temp.

Power๏ผˆKW)

Voltage

Max.Vacuum

DW-QHM-223

200*200*300

1350โ„ƒ

42

380V

7ร—10-4 Pa

DW-QHM-334

300*300*400

1350โ„ƒ

72

380V

DW-QHM-446

400*400*600

1350โ„ƒ

120

380V

DW-QHM-557

500*500*700

1350โ„ƒ

160

380V

DW-QHM-669

600*600*900

1350โ„ƒ

225

380V

 

 

MoSi2 Heater High Temperature Vacuum Furnace up to 1700โ„ƒ

Model

Max Temp.

(โ„ƒ)

Chamber size
(WxHxD) (mm)

Heating element

Capacity
(L)

Power
(KW)

Max.

Vacuum

DW-17VF-1

1700

100*100*100

MoSi2 heater

1

1.5

7ร—10-3 Pa

(7ร—10-5 mbar)

DW-17VF-5

1700

150*150*200

MoSi2 heater

4.5

5

DW-17VF-12

1700

200*200*300

MoSi2 heater

12

8

DW-17VF-36

1700

300*300*400

MoSi2 heater

36

12

DW-17VF-80

1700

400*400*600

MoSi2 heater

96

30

DW-17VF-175

1700

500*500*700

MoSi2 heater

175

45

DW-17VF-324

1700

600*600*900

MoSi2 heater

324

70

 

 

High Temperature Graphite Vacuum Furnace up to 2200โ„ƒ

Model

Heating Zone

(Dia.* Height)

Temperature

Power

Voltage

Max. Vacuum

DW-22STV-20

ฮฆ80ร—100mm

2200โ„ƒ

20kW

380V

7ร—10-3 Pa

(7ร—10-5 mbar)

DW-22STV-25

ฮฆ90ร—120mm

2200โ„ƒ

25kW

380V

DW-22STV-40

ฮฆ140ร—160mm

2200โ„ƒ

40kW

380V

DW-22STV-50

ฮฆ160ร—200mm

2200โ„ƒ

50kW

380V

DW-22STV-60

ฮฆ260ร—270mm

2200โ„ƒ

60kW

380V

DW-22STV-100

ฮฆ320ร—320mm

2200โ„ƒ

100kW

380V

 

For precision thermal processing, a laboratory vacuum furnace is the gold standard. Whether youโ€™re engaged in fundamental materials research, developing advanced alloys, or producing high-purity components, investing in vacuum heat treatment technology ensures reliable, scalable, and contamination-free results.

For more information on laboratory vacuum furnaces and custom configurations for your heat treatment requirements, consult reputable manufacturers or request detailed technical guidance tailored to your application.


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